Information card for entry 4338445

Structure parameters

• Formula: H29 K3 Mn3 Na O50 Si W9
• Calculated formula: K2.8 Mn3 Na1.25 O49 Si W9
• Title of publication: Synthesis and characterization of multinuclear manganese-containing tungstosilicates.
• Authors of publication: Al-Oweini, Rami; Bassil, Bassem S.; Friedl, Jochen; Kottisch, Veronika; Ibrahim, Masooma; Asano, Marie; Keita, Bineta; Novitchi, Ghenadie; Lan, Yanhua; Powell, Annie; Stimming, Ulrich; Kortz, Ulrich
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 11
• Pages of publication: 5663 - 5673
• a: 21.1404 ± 0.0014 Å
• b: 21.0962 ± 0.0012 Å
• c: 23.9958 ± 0.0014 Å
• α: 90°
• β: 105.286 ± 0.003°
• γ: 90°
• Cell volume: 10323.1 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0704
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.1526
• Weighted residual factors for all reflections included in the refinement: 0.1603
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No