Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F13.
Authors of publication
Yeon, Jeongho; Smith, Mark D.; Tapp, Joshua; Möller, Angela; Zur Loye, Hans-Conrad
Journal of publication
Inorganic chemistry
Year of publication
2014
Journal volume
53
Journal issue
12
Pages of publication
6289 - 6298
a
15.1426 ± 0.0008 Å
b
15.1426 ± 0.0008 Å
c
10.3856 ± 0.001 Å
α
90°
β
90°
γ
120°
Cell volume
2062.4 ± 0.3 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
3
Space group number
148
Hermann-Mauguin space group symbol
R -3
Hall space group symbol
-R 3
Residual factor for all reflections
0.0492
Residual factor for significantly intense reflections
0.0395
Weighted residual factors for significantly intense reflections
0.1008
Weighted residual factors for all reflections included in the refinement
0.1055
Goodness-of-fit parameter for all reflections included in the refinement
