Crystallography Open Database

Information card for entry 4338610

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Structure parameters

Formula	C30 H52 Li2 N4
Calculated formula	C30 H52 Li2 N4
SMILES	[Li]1[NH](c2c(cccc2C(C)C)C(C)C)[Li]([NH]1c1c(cccc1C(C)C)C(C)C)[N](C)(C)CC[N](C)(C)[Li]1[NH](c2c(cccc2C(C)C)C(C)C)[Li]([NH]1c1c(cccc1C(C)C)C(C)C)[N](C)(C)CCN(C)C
Title of publication	Donor-Dictated Interlocking Co-Complexation Reactions of LiNHDipp with Dimethylzinc: Synthesis and Structures of New Methyl(amido)zincates
Authors of publication	Clegg, William; Graham, David V.; Herd, Emma; Hevia, Eva; Kennedy, Alan R.; McCall, Matthew D.; Russo, Luca
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Journal issue	12
Pages of publication	5320 - 5327
a	8.4634 ± 0.0005 Å
b	9.1374 ± 0.001 Å
c	10.9932 ± 0.0007 Å
α	75.394 ± 0.009°
β	87.935 ± 0.006°
γ	72.64 ± 0.007°
Cell volume	784.49 ± 0.12 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0543
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.1033
Weighted residual factors for all reflections included in the refinement	0.1104
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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