Information card for entry 4338741

Structure parameters

• Formula: C42 H35 Cu8 N9 O104 W22
• Calculated formula: C42 H35 Cu8 N9 O104 W22
• Title of publication: Novel Isopolyoxotungstate [H2W11O38](8-) Based Metal Organic Framework: As Lewis Acid Catalyst for Cyanosilylation of Aromatic Aldehydes.
• Authors of publication: Han, Qiuxia; Sun, Xueping; Li, Jie; Ma, Pengtao; Niu, Jingyang
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 6107 - 6112
• a: 10.0082 ± 0.0014 Å
• b: 21.721 ± 0.003 Å
• c: 14.825 ± 0.002 Å
• α: 90°
• β: 108.029 ± 0.002°
• γ: 90°
• Cell volume: 3064.5 ± 0.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1187
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No