Information card for entry 4338771

Structure parameters

• Formula: C38 H68 N3 O2 Si6 U
• Calculated formula: C37.3 H67.9 N3 O2 Si6 U
• Title of publication: The inverse trans influence in a family of pentavalent uranium complexes.
• Authors of publication: Lewis, Andrew J.; Mullane, Kimberly C.; Nakamaru-Ogiso, Eiko; Carroll, Patrick J.; Schelter, Eric J.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 13
• Pages of publication: 6944 - 6953
• a: 27.051 ± 0.002 Å
• b: 11.9471 ± 0.0009 Å
• c: 18.0215 ± 0.0013 Å
• α: 90°
• β: 127.293 ± 0.004°
• γ: 90°
• Cell volume: 4633.4 ± 0.6 ų
• Cell temperature: 143 ± 1 K
• Ambient diffraction temperature: 143 ± 1 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.1182
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No