Information card for entry 4338977

Structure parameters

• Formula: C74 H106 Cl4 Ga2 N4 O4 Zn2
• Calculated formula: C74 H106 Cl4 Ga2 N4 O4 Zn2
• Title of publication: Synthesis and structure of new compounds with Zn-Ga bonds: insertion of the gallium(I) bisimidinate Ga(DDP) into Zn-X (X = CH3, Cl) and the homoleptic complex cation [Zn(GaCp*)4]2+.
• Authors of publication: Kempter, Andreas; Gemel, Christian; Cadenbach, Thomas; Fischer, Roland A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 22
• Pages of publication: 9481 - 9487
• a: 10.2208 ± 0.0004 Å
• b: 19.127 ± 0.0014 Å
• c: 10.7564 ± 0.0007 Å
• α: 90°
• β: 90.242 ± 0.004°
• γ: 90°
• Cell volume: 2102.8 ± 0.2 ų
• Cell temperature: 105 ± 2 K
• Ambient diffraction temperature: 105 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1269
• Residual factor for significantly intense reflections: 0.0596
• Weighted residual factors for significantly intense reflections: 0.1382
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 0.817
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No