Information card for entry 4339063

Structure parameters

• Formula: C40 H58 As8 N16 Ni2 O43 V14
• Calculated formula: C40 H56 As8 N16 Ni2 O43 V14
• Title of publication: High-dimensional assembly depending on polyoxoanion templates, metal ion coordination geometries, and a flexible bis(imidazole) ligand.
• Authors of publication: Dong, Bao-xia; Peng, Jun; Gómez-García, Carlos J; Benmansour, Samia; Jia, Heng-qing; Hu, Ning-hai
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 15
• Pages of publication: 5933 - 5941
• a: 20.9245 ± 0.0004 Å
• b: 20.9245 ± 0.0004 Å
• c: 40.6114 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 17781.1 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 142
• Hermann-Mauguin space group symbol: I 41/a c d :2
• Hall space group symbol: -I 4bd 2c
• Residual factor for all reflections: 0.0904
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1461
• Weighted residual factors for all reflections included in the refinement: 0.168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No