Information card for entry 4339146

Structure parameters

• Formula: C36 H42 Cl2 O4 P2 Pd
• Calculated formula: C36 H42 Cl2 O4 P2 Pd
• Title of publication: New tertiary phosphines from cinnamaldehydes and diphenylphosphine.
• Authors of publication: Moiseev, Dmitry V.; Patrick, Brian O.; James, Brian R.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 26
• Pages of publication: 11467 - 11474
• a: 14.7439 ± 0.0006 Å
• b: 21.8538 ± 0.0009 Å
• c: 21.9153 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7061.3 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0889
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1023
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.118
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No