Information card for entry 4339160

Structure parameters

• Formula: C63 H51 Cl2 N5 Os P2
• Calculated formula: C63 H51 Cl2 N5 Os P2
• Title of publication: cis-Dicyanoosmium(II) diimine complexes bearing phosphine or sulfoxide ligands: spectroscopic and luminescent studies.
• Authors of publication: Lai, Siu-Wai; Chan, Queenie K.-W.; Zhu, Nianyong; Che, Chi-Ming
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 26
• Pages of publication: 11003 - 11016
• a: 12.015 ± 0.002 Å
• b: 13.223 ± 0.003 Å
• c: 17.861 ± 0.004 Å
• α: 83.28 ± 0.03°
• β: 87.84 ± 0.03°
• γ: 75.57 ± 0.03°
• Cell volume: 2729.1 ± 1.1 ų
• Cell temperature: 301 ± 2 K
• Ambient diffraction temperature: 301 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0355
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0866
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No