Information card for entry 4339253

Structure parameters

• Formula: C47 H54 B2 F10 N8 O3 Zn2
• Calculated formula: C47 H54 B2 F10 N8 O3 Zn2
• Title of publication: Binuclear fluoro-bridged zinc and cadmium complexes of a schiff base expanded porphyrin: fluoride abstraction from the tetrafluoroborate anion.
• Authors of publication: Tomat, Elisa; Cuesta, Luciano; Lynch, Vincent M.; Sessler, Jonathan L.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 16
• Pages of publication: 6224 - 6226
• a: 27.6016 ± 0.0003 Å
• b: 10.8804 ± 0.0002 Å
• c: 20.1887 ± 0.0003 Å
• α: 90°
• β: 126.536 ± 0.001°
• γ: 90°
• Cell volume: 4871.52 ± 0.14 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1481
• Weighted residual factors for all reflections included in the refinement: 0.1574
• Goodness-of-fit parameter for all reflections included in the refinement: 1.184
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No