Information card for entry 4339440

Structure parameters

• Formula: Cu10 Ge4 H64 K10 N12 Na14 O162 W34
• Calculated formula: Cu10 Ge4 K10 N12 Na14 O162 W34
• Title of publication: Two multi-copper-containing heteropolyoxotungstates constructed from the lacunary Keggin polyoxoanion and the high-nuclear spin cluster.
• Authors of publication: Zhang, Zhiming; Qi, Yanfei; Qin, Chao; Li, Yangguang; Wang, Enbo; Wang, Xinlong; Su, Zhongmin; Xu, Lin
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 20
• Pages of publication: 8162 - 8169
• a: 12.309 ± 0.003 Å
• b: 17.979 ± 0.004 Å
• c: 21.586 ± 0.004 Å
• α: 103.05 ± 0.03°
• β: 100.04 ± 0.03°
• γ: 108.04 ± 0.03°
• Cell volume: 4268 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1208
• Residual factor for significantly intense reflections: 0.0758
• Weighted residual factors for significantly intense reflections: 0.1753
• Weighted residual factors for all reflections included in the refinement: 0.2041
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No