Information card for entry 4339487

Structure parameters

• Formula: C80 H56 Cl8 N8 Ni8 O8.5
• Calculated formula: C80 H56 Cl8 N8 Ni8 O8.5
• Title of publication: One-pot synthesis of Schiff-base-containing Ni8 clusters: solvothermal synthesis, structure, and magnetic properties.
• Authors of publication: Luo, Feng; Zheng, Ji-min; Kurmoo, Mohamedally
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 21
• Pages of publication: 8448 - 8450
• a: 12.543 ± 0.003 Å
• b: 12.896 ± 0.003 Å
• c: 13.782 ± 0.003 Å
• α: 97.06 ± 0.03°
• β: 105.64 ± 0.03°
• γ: 115.01 ± 0.03°
• Cell volume: 1872.4 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1193
• Residual factor for significantly intense reflections: 0.0688
• Weighted residual factors for significantly intense reflections: 0.1813
• Weighted residual factors for all reflections included in the refinement: 0.2122
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No