Information card for entry 4339522

Structure parameters

• Formula: C114 H261 Cl4 N7 O74 Si2 W20 Zr2
• Calculated formula: C114 Cl4 N7 O74 Si2 W20 Zr2
• Title of publication: Synthesis and structural characterization of a gamma-Keggin-type dimeric silicotungstate with a bis(mu-hydroxo) dizirconium core [(gamma-SiW10O36)2Zr2(mu-OH)2]10-.
• Authors of publication: Yamaguchi, Syuhei; Kikukawa, Yuji; Tsuchida, Kazutaka; Nakagawa, Yoshinao; Uehara, Kazuhiro; Yamaguchi, Kazuya; Mizuno, Noritaka
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 21
• Pages of publication: 8502 - 8504
• a: 29.4764 ± 0.0007 Å
• b: 35.6269 ± 0.0008 Å
• c: 19.0523 ± 0.0003 Å
• α: 90°
• β: 108.747 ± 0.0008°
• γ: 90°
• Cell volume: 18946.4 ± 0.7 ų
• Cell temperature: 153.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for all reflections included in the refinement: 0.202
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No