Information card for entry 4339598

Structure parameters

• Formula: C98 H158 K2 N2 Ni2 O16 P2 S6 Si6
• Calculated formula: C98 H158 K2 N2 Ni2 O16 P2 S6 Si6
• Title of publication: Mononuclear Ni(II)-thiolate complexes with pendant thiol and dinuclear Ni(III/II)-thiolate complexes with Ni...Ni interaction regulated by the oxidation levels of nickels and the coordinated ligands.
• Authors of publication: Lee, Chien-Ming; Chiou, Tzung-Wen; Chen, Hsin-Hung; Chiang, Chao-Yi; Kuo, Ting-Shen; Liaw, Wen-Feng
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 21
• Pages of publication: 8913 - 8923
• a: 13.6148 ± 0.0004 Å
• b: 15.3156 ± 0.0004 Å
• c: 18.099 ± 0.0006 Å
• α: 112.955 ± 0.001°
• β: 109.818 ± 0.001°
• γ: 93.002 ± 0.001°
• Cell volume: 3194.22 ± 0.17 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1322
• Residual factor for significantly intense reflections: 0.0973
• Weighted residual factors for significantly intense reflections: 0.2519
• Weighted residual factors for all reflections included in the refinement: 0.2733
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No