Information card for entry 4339740

Structure parameters

• Formula: C48 H28 Ca0.18 N4 O10 Sm
• Calculated formula: C48 H28 Ca0.181 N4 O10 Sm
• Title of publication: Porphyrin framework solids. Synthesis and structure of hybrid coordination polymers of tetra(carboxyphenyl)porphyrins and lanthanide-bridging ions.
• Authors of publication: Muniappan, Sankar; Lipstman, Sophia; George, Sumod; Goldberg, Israel
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 14
• Pages of publication: 5544 - 5554
• a: 9.6187 ± 0.0003 Å
• b: 13.8934 ± 0.0006 Å
• c: 17.2345 ± 0.0007 Å
• α: 98.058 ± 0.002°
• β: 90.457 ± 0.002°
• γ: 90.599 ± 0.003°
• Cell volume: 2280.19 ± 0.15 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.067
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1121
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No