Information card for entry 4339751

Structure parameters

• Formula: F11 K2 O27 Tc9
• Calculated formula: F11 K2 O27 Tc9
• SMILES: [Tc]12(=O)(=O)(=O)[F][Tc]3(=O)(=O)(=O)[F][Tc](=O)(=O)(=O)([F]1)[F]23.[Tc]12(=O)(=O)(=O)[F][Tc]3(=O)(=O)(=O)[F][Tc](=O)(=O)(=O)([F]1)[F]23.[Tc](=O)(=O)(=O)F.[Tc](=O)(=O)(=O)F.[Tc](=O)(=O)(=O)F.[K+].[K+]
• Title of publication: Technetium fluoride trioxide, TcO3F, preparation and properties.
• Authors of publication: Supeł, Joanna; Abram, Ulrich; Hagenbach, Adelheid; Seppelt, Konrad
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 14
• Pages of publication: 5591 - 5595
• a: 8.2721 ± 0.001 Å
• b: 14.1477 ± 0.0011 Å
• c: 24.749 ± 0.003 Å
• α: 90°
• β: 92.719 ± 0.01°
• γ: 90°
• Cell volume: 2893.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0677
• Weighted residual factors for all reflections included in the refinement: 0.077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No