Information card for entry 4339798

Structure parameters

• Common name: [(C6H11NC)12Rh3Cl2][(C6H11NC)8Rh2]][(C6H11NC)4Rh](Cl6).16H2O.3benzene
• Formula: C186 H314 Cl6 N24 O16 Rh6
• Calculated formula: C186 H282 Cl6 N24 O16 Rh6
• Title of publication: Adventures in crystallization. Crystalline salts containing one, two, or even three chemically distinct cations obtained from solutions of [(cyclohexyl isocyanide)(4)Rh(I)]+.
• Authors of publication: Tran, Ngon T.; Stork, Jay R.; Pham, David; Chancellor, Christopher J.; Olmstead, Marilyn M.; Fettinger, James C.; Balch, Alan L.
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 19
• Pages of publication: 7998 - 8007
• a: 21.101 ± 0.004 Å
• b: 20.105 ± 0.003 Å
• c: 23.857 ± 0.004 Å
• α: 90°
• β: 91.086 ± 0.004°
• γ: 90°
• Cell volume: 10119 ± 3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.207
• Residual factor for significantly intense reflections: 0.1227
• Weighted residual factors for significantly intense reflections: 0.2888
• Weighted residual factors for all reflections included in the refinement: 0.3487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No