Information card for entry 4339829

Structure parameters

• Formula: C46 H45 F6 N Ni O6 P4 S2
• Calculated formula: C46 H45 F6 N Ni O6 P4 S2
• Title of publication: Synthesis, structure, and electrochemistry of di- and zerovalent nickel, palladium, and platinum monomers and dimers derived from an enantiopure (S,S)-tetra(tertiary phosphine).
• Authors of publication: Kitto, Heather J.; Rae, A. David; Webster, Richard D.; Willis, Anthony C.; Wild, S. Bruce
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 19
• Pages of publication: 8059 - 8070
• a: 13.2784 ± 0.0001 Å
• b: 19.324 ± 0.0002 Å
• c: 37.3338 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9579.55 ± 0.16 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for all reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.0463
• Weighted residual factors for all reflections included in the refinement: 0.0463
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1872
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No