Information card for entry 4340049

Structure parameters

• Chemical name: Eu(III)[15-MC Zn(II),picHA-5](NO3)3(py)4
• Formula: C50 H44 Eu N17 O21 Zn5
• Calculated formula: C50 H40 Eu N17 O20.99 Zn5
• Title of publication: Solvent dependent assembly of lanthanide metallacrowns using building blocks with incompatible symmetry preferences.
• Authors of publication: Jankolovits, Joseph; Kampf, Jeff W.; Pecoraro, Vincent L.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 14
• Pages of publication: 7534 - 7546
• a: 45.3648 ± 0.0006 Å
• b: 45.3648 ± 0.0006 Å
• c: 12.0304 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 24758.1 ± 1.9 ų
• Cell temperature: 85 ± 2 K
• Ambient diffraction temperature: 85 ± 2 K
• Number of distinct elements: 6
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for significantly intense reflections: 0.1608
• Weighted residual factors for all reflections included in the refinement: 0.1648
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No