Information card for entry 4340773

Structure parameters

• Formula: C50 H96 Fe K N2 O8 Si2
• Calculated formula: C50 H96 Fe K N2 O8 Si2
• Title of publication: Synthesis, structure, and magnetic and electrochemical properties of quasi-linear and linear iron(i), cobalt(i), and nickel(i) amido complexes.
• Authors of publication: Lin, Chun-Yi; Fettinger, James C.; Grandjean, Fernande; Long, Gary J.; Power, Philip P.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 17
• Pages of publication: 9400 - 9406
• a: 49.241 ± 0.005 Å
• b: 9.8527 ± 0.0009 Å
• c: 25.173 ± 0.002 Å
• α: 90°
• β: 105.665 ± 0.0014°
• γ: 90°
• Cell volume: 11759.2 ± 1.9 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1041
• Weighted residual factors for all reflections included in the refinement: 0.1104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No