Information card for entry 4340794

Structure parameters

• Formula: C38 H48 F3 Ge3 Mn3 N2 O18 S
• Calculated formula: C38 H48 F3 Ge3 Mn3 N2 O18 S
• Title of publication: Conversion of a Monodentate Amidinate-Germylene Ligand into Chelating Imine-Germanate Ligands (on Mononuclear Manganese Complexes).
• Authors of publication: Cabeza, Javier A.; García-Álvarez, Pablo; Pérez-Carreño, Enrique; Polo, Diego
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 16
• Pages of publication: 8735 - 8741
• a: 22.1574 ± 0.0003 Å
• b: 9.5888 ± 0.0002 Å
• c: 25.3889 ± 0.0004 Å
• α: 90°
• β: 96.572 ± 0.015°
• γ: 90°
• Cell volume: 5358.8 ± 0.2 ų
• Cell temperature: 152 ± 2 K
• Ambient diffraction temperature: 152 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.0952
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No