Information card for entry 4340976

Structure parameters

• Formula: C18 H54 N3 P Si6
• Calculated formula: C18 H54 N3 P Si6
• Title of publication: Structural distortions in M[E(SiMe₃)₂]₃ complexes (M = group 15, f-element; E = N, CH): is three a crowd?
• Authors of publication: Boyde, Nicholas C.; Chmely, Stephen C.; Hanusa, Timothy P.; Rheingold, Arnold L.; Brennessel, William W.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 9703 - 9714
• a: 8.9279 ± 0.0005 Å
• b: 19.0519 ± 0.001 Å
• c: 20.6374 ± 0.001 Å
• α: 115.085 ± 0.0012°
• β: 97.9463 ± 0.0013°
• γ: 95.3845 ± 0.0015°
• Cell volume: 3102.8 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.054
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0967
• Weighted residual factors for all reflections included in the refinement: 0.1034
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No