Crystallography Open Database

Information card for entry 4340979

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Coordinates	4340979.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H56 Cl4 N4 O U
Calculated formula	C40 H56 Cl4 N4 O U
Title of publication	Preparation and reactivity of the versatile uranium(IV) imido complexes U(NAr)Cl₂(R₂bpy)₂ (R = Me, (t)Bu) and U(NAr)Cl₂(tppo)₃.
Authors of publication	Jilek, Robert E.; Tomson, Neil C.; Shook, Ryan L.; Scott, Brian L.; Boncella, James M.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	18
Pages of publication	9818 - 9826
a	16.5422 ± 0.0011 Å
b	11.554 ± 0.0008 Å
c	25.5297 ± 0.0018 Å
α	90°
β	94.701 ± 0.001°
γ	90°
Cell volume	4863 ± 0.6 Å³
Cell temperature	120 ± 1 K
Ambient diffraction temperature	120 ± 1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0472
Residual factor for significantly intense reflections	0.0319
Weighted residual factors for significantly intense reflections	0.0696
Weighted residual factors for all reflections included in the refinement	0.0735
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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