Information card for entry 4341020

Structure parameters

• Formula: Cl13 P U2
• Calculated formula: Cl13 P U2
• Title of publication: The synthesis and characterization of four new uranium(IV) chlorophosphates: UCl₄(POCl₃), [U₂Cl₉][PCl₄], UCl₃(PO₂Cl₂), and U₂Cl₈(POCl₃).
• Authors of publication: Ward, Matthew D.; Chan, Ian Y.; Lebègue, Sébastien; Ibers, James A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 9969 - 9975
• a: 8.3695 ± 0.0002 Å
• b: 13.419 ± 0.0003 Å
• c: 16.9609 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1904.88 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0508
• Weighted residual factors for all reflections included in the refinement: 0.0542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.235
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No