Information card for entry 4341144

Structure parameters

• Formula: C75.75 H71.5 B2 N12 O3.25 Rh2
• Calculated formula: C75.75 H71.5 B2 N12 O3.25 Rh2
• Title of publication: Hemilabile and Bimetallic Coordination in Rh and Ir Complexes of NCN Pincer Ligands.
• Authors of publication: Mancano, Giulia; Page, Michael J.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 19
• Pages of publication: 10159 - 10170
• a: 12.6272 ± 0.0004 Å
• b: 26.3368 ± 0.0008 Å
• c: 22.9366 ± 0.0007 Å
• α: 90°
• β: 91.129 ± 0.001°
• γ: 90°
• Cell volume: 7626.3 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1553
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1449
• Weighted residual factors for all reflections included in the refinement: 0.1834
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No