Information card for entry 4341316

Structure parameters

• Formula: H142 Na16 O183 P4 Pd4 W30
• Calculated formula: Na9 O143.76 P4 Pd4.02 W30
• Title of publication: Tetrapalladium-Containing Polyoxotungstate [Pd(II)4(α-P2W15O56)2](16-): A Comparative Study.
• Authors of publication: Izarova, Natalya V.; Maksimovskaya, Raisa I.; Willbold, Sabine; Kögerler, Paul
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 21
• Pages of publication: 11778 - 11784
• a: 14.0333 ± 0.0003 Å
• b: 14.0985 ± 0.0003 Å
• c: 25.2703 ± 0.0005 Å
• α: 83.9425 ± 0.0017°
• β: 76.516 ± 0.0019°
• γ: 60.514 ± 0.002°
• Cell volume: 4231.89 ± 0.18 ų
• Cell temperature: 120 ± 0.14 K
• Ambient diffraction temperature: 120 ± 0.14 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1829
• Weighted residual factors for all reflections included in the refinement: 0.1874
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No