Information card for entry 4341345

Structure parameters

• Chemical name: [Rh(3,6-DBSQ-4,5-(N,N-DEN))(CO)2]
• Formula: C20 H26 N2 O4 Rh
• Calculated formula: C20 H26 N2 O4 Rh
• Title of publication: Multifunctional one-dimensional rhodium(i)-semiquinonato complex: substituent effects on crystal structures and solid-state properties.
• Authors of publication: Mitsumi, Minoru; Ohtake, Shoji; Kakuno, Yuki; Komatsu, Yuuki; Ozawa, Yoshiki; Toriumi, Koshiro; Yasuda, Nobuhiro; Azuma, Nobuaki; Miyazaki, Yuji
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 21
• Pages of publication: 11710 - 11720
• a: 6.1926 ± 0.0004 Å
• b: 16.3109 ± 0.001 Å
• c: 21.7617 ± 0.0016 Å
• α: 110.035 ± 0.0016°
• β: 97.032 ± 0.002°
• γ: 93.212 ± 0.002°
• Cell volume: 2038.2 ± 0.2 ų
• Cell temperature: 250 ± 1 K
• Ambient diffraction temperature: 250 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1284
• Weighted residual factors for all reflections included in the refinement: 0.1522
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.83077 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No