Information card for entry 4341633

Structure parameters

• Formula: C8 H88.8 Co2.2 K3 N4 Na7 O115 Te2 W19.8
• Calculated formula: C8 H6 Co2.23 K3 N4 Na5.6 O107.2 Te2 W19.77
• Title of publication: Functionalization of krebs-type polyoxometalates with n,o-chelating ligands: a systematic study.
• Authors of publication: Artetxe, Beñat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Pache, Aroa; Martín-Caballero, Jagoba; Gutiérrez-Zorrilla, Juan M
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 1
• Pages of publication: 241 - 252
• a: 12.1725 ± 0.0004 Å
• b: 13.566 ± 0.0004 Å
• c: 17.1425 ± 0.0005 Å
• α: 91.535 ± 0.003°
• β: 98.099 ± 0.003°
• γ: 107.057 ± 0.003°
• Cell volume: 2672.32 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1286
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No