Information card for entry 4341675

Structure parameters

• Formula: C99 H102 F3 N2 O8 S Si2 U
• Calculated formula: C99 H102 F3 N2 O8 S Si2 U
• Title of publication: Reductive Silylation of the Uranyl Ion with Ph3SiOTf
• Authors of publication: Pedrick, Elizabeth A.; Wu, Guang; Hayton, Trevor W.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2014
• Pages of publication: 141111154001001
• a: 13.2871 ± 0.0002 Å
• b: 14.1711 ± 0.0003 Å
• c: 15.2003 ± 0.0003 Å
• α: 63.915 ± 0.001°
• β: 73.8 ± 0.001°
• γ: 69.232 ± 0.001°
• Cell volume: 2377.6 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.091
• Weighted residual factors for all reflections included in the refinement: 0.0914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No