Synthesis and Characterization of the Platinum-Substituted Keggin Anion α-H2SiPtW11O40(4-)
Authors of publication
Klonowski, Peter; Goloboy, James C.; Uribe-Romo, Fernando J; Sun, Furong; Zhu, Lingyang; Gándara, Felipe; Wills, Corinne; Errington, R. John; Yaghi, Omar M.; Klemperer, Walter G.
Journal of publication
Inorganic chemistry
Year of publication
2014
Pages of publication
141119142641005
a
17.669 ± 0.002 Å
b
17.669 ± 0.002 Å
c
17.669 ± 0.002 Å
α
90°
β
90°
γ
90°
Cell volume
5516.1 ± 1.1 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
229
Hermann-Mauguin space group symbol
I m -3 m
Hall space group symbol
-I 4 2 3
Residual factor for all reflections
0.0392
Residual factor for significantly intense reflections
0.0361
Weighted residual factors for significantly intense reflections
0.121
Weighted residual factors for all reflections included in the refinement
0.1232
Goodness-of-fit parameter for all reflections included in the refinement
