Information card for entry 4342008

Structure parameters

• Formula: C6 H44 B13 Co N6 O31
• Calculated formula: C6 H44 B13 Co N6 O31
• Title of publication: A New Decaoxidooctaborate(2-) Anion, [B8O10(OH)6](2-): Synthesis and Characterization of [Co(en)3][B5O6(OH)4][B8O10(OH)6)]·5H2O (en = 1,2-Diaminoethane).
• Authors of publication: Altahan, Mohammed A.; Beckett, Michael A.; Coles, Simon J.; Horton, Peter N.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 2
• Pages of publication: 412 - 414
• a: 11.2993 ± 0.0008 Å
• b: 11.5139 ± 0.0008 Å
• c: 13.7574 ± 0.001 Å
• α: 88.272 ± 0.004°
• β: 76.22 ± 0.004°
• γ: 88.984 ± 0.004°
• Cell volume: 1737.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1182
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No