Information card for entry 4342106

Structure parameters

• Formula: B22 H32 O55 Pr4
• Calculated formula: B22 O55 Pr4
• Title of publication: Ionothermal Synthesis of Tetranuclear Borate Clusters Containing f- and p-Block Metals.
• Authors of publication: Parker, T. Gannon; Chown, Amanda L.; Beehler, Austin; Pubbi, Divya; Cross, Justin N.; Albrecht-Schmitt, Thomas E
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 2
• Pages of publication: 570 - 575
• a: 18.0098 ± 0.0007 Å
• b: 18.0098 ± 0.0007 Å
• c: 18.0098 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5841.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 197
• Hermann-Mauguin space group symbol: I 2 3
• Hall space group symbol: I 2 2 3
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1763
• Weighted residual factors for all reflections included in the refinement: 0.1783
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No