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Information card for entry 4342183
Preview
Coordinates | 4342183.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 1,3-Di-tert-butyl-2,4-bis(phenylethynyl)-[1,3,2,4] diazadiphosphetidine |
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Formula | C24 H28 N2 P2 |
Calculated formula | C24 H28 N2 P2 |
SMILES | P1(N(P(N1C(C)(C)C)C#Cc1ccccc1)C(C)(C)C)C#Cc1ccccc1 |
Title of publication | Construction of the First Rhodium(I) Cyclic Pentameric Structure [Rh(CO)Cl{(μ-N(t)BuP)2(C≡CPh)2}]5 Using (Phenylethynyl)cyclodiphosphazanes. |
Authors of publication | Siddiqui, Mujahuddin M.; Mague, Joel T.; Balakrishna, Maravanji S. |
Journal of publication | Inorganic chemistry |
Year of publication | 2015 |
Journal volume | 54 |
Journal issue | 4 |
Pages of publication | 1200 - 1202 |
a | 15.6716 ± 0.0011 Å |
b | 10.4009 ± 0.0007 Å |
c | 15.5875 ± 0.001 Å |
α | 90° |
β | 115.172 ± 0.001° |
γ | 90° |
Cell volume | 2299.5 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0444 |
Residual factor for significantly intense reflections | 0.0362 |
Weighted residual factors for significantly intense reflections | 0.0944 |
Weighted residual factors for all reflections included in the refinement | 0.1019 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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