Crystallography Open Database

Information card for entry 4342274

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Coordinates	4342274.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30.5 H40 Br3 N3 Si
Calculated formula	C30.5 H40 Br3 N3 Si
Title of publication	Contrasting reactivities of silicon and germanium complexes supported by an N-heterocyclic guanidine ligand.
Authors of publication	Lui, Melanie W.; Merten, Christian; Ferguson, Michael J.; McDonald, Robert; Xu, Yunjie; Rivard, Eric
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	4
Pages of publication	2040 - 2049
a	9.3324 ± 0.0007 Å
b	9.5737 ± 0.0007 Å
c	19.7142 ± 0.0014 Å
α	91.4794 ± 0.001°
β	96.1262 ± 0.001°
γ	111.416 ± 0.0009°
Cell volume	1626.4 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0675
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0745
Weighted residual factors for all reflections included in the refinement	0.0837
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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