Information card for entry 4342447

Structure parameters

• Formula: C56 H63 B Cl2 N2 O3 P2 Ru
• Calculated formula: C56 H63 B Cl2 N2 O3 P2 Ru
• Title of publication: Hydrolysis of Coordinated Diazoalkanes To Yield Side-On 1,2-Diazene Derivatives.
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Botter, Alessandra; Castro, Jesús
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 5
• Pages of publication: 2091
• a: 12.9766 ± 0.0005 Å
• b: 18.2347 ± 0.0007 Å
• c: 23.2723 ± 0.0008 Å
• α: 90°
• β: 102.958 ± 0.0013°
• γ: 90°
• Cell volume: 5366.6 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.1483
• Weighted residual factors for all reflections included in the refinement: 0.1576
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No