Information card for entry 4342698

Structure parameters

• Formula: C7 H9 B F N4 Na Si
• Calculated formula: C7 H9 B F N4 Na Si
• Title of publication: Syntheses of Tricyanofluoroborates M[BF(CN)3] (M = Na, K): (CH3)3SiCl Catalysis, Countercation Effect, and Reaction Intermediates.
• Authors of publication: Sprenger, Jan A. P.; Landmann, Johannes; Drisch, Michael; Ignat'ev, Nikolai; Finze, Maik
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 7
• Pages of publication: 3403 - 3412
• a: 14.6004 ± 0.0009 Å
• b: 8.8498 ± 0.0007 Å
• c: 10.0689 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1301.01 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0254
• Residual factor for significantly intense reflections: 0.0228
• Weighted residual factors for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.0598
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No