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Information card for entry 4342774
Preview
Coordinates | 4342774.cif |
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Original paper (by DOI) | HTML |
Formula | C33 H54 Cl Co N3 Si2 |
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Calculated formula | C33 H54 Cl Co N3 Si2 |
SMILES | [Co](Cl)(N([Si](C)(C)C)[Si](C)(C)C)=C1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C |
Title of publication | Protonolysis and amide exchange reactions of a three-coordinate cobalt amide complex supported by an N-heterocyclic carbene ligand. |
Authors of publication | Hansen, Christopher B.; Jordan, Richard F.; Hillhouse, Gregory L. |
Journal of publication | Inorganic chemistry |
Year of publication | 2015 |
Journal volume | 54 |
Journal issue | 10 |
Pages of publication | 4603 - 4610 |
a | 10.782 ± 0.0005 Å |
b | 17.8049 ± 0.0007 Å |
c | 19.6609 ± 0.0009 Å |
α | 90° |
β | 101.804 ± 0.002° |
γ | 90° |
Cell volume | 3694.5 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0481 |
Residual factor for significantly intense reflections | 0.0316 |
Weighted residual factors for significantly intense reflections | 0.0981 |
Weighted residual factors for all reflections included in the refinement | 0.1113 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.847 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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