Information card for entry 4342848

Structure parameters

• Formula: C27 H32 N2 O1.75 Pd S
• Calculated formula: C27 H32 N2 O1.75 Pd S
• Title of publication: Palladium(II) Complex of a Redox-Active Amidophenolate-Based O,N,S,N Ligand: Its Monocation and Dication and Reactivity with PPh3.
• Authors of publication: Ali, Akram; Barman, Suman K.; Mukherjee, Rabindranath
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 11
• Pages of publication: 5182 - 5194
• a: 13.003 ± 0.005 Å
• b: 10.137 ± 0.005 Å
• c: 18.385 ± 0.005 Å
• α: 90 ± 0.005°
• β: 92.427 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 2421.2 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.0996
• Weighted residual factors for all reflections included in the refinement: 0.1365
• Goodness-of-fit parameter for all reflections included in the refinement: 0.92
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No