Information card for entry 4343010

Structure parameters

• Formula: C10 H19 B11 Cl11 P Pd
• Calculated formula: C10 H19 B11 Cl11 P Pd
• Title of publication: Synthesis and reactivity of a zwitterionic palladium allyl complex supported by a perchlorinated carboranyl phosphine.
• Authors of publication: Estrada, Jess; Woen, David H.; Tham, Fook S.; Miyake, Garret M.; Lavallo, Vincent
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 11
• Pages of publication: 5142 - 5144
• a: 9.6042 ± 0.0004 Å
• b: 20.1819 ± 0.0009 Å
• c: 14.5495 ± 0.0007 Å
• α: 90°
• β: 94.726 ± 0.001°
• γ: 90°
• Cell volume: 2810.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0876
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No