Information card for entry 4343608

Structure parameters

• Formula: C220 H350 Ge18 Hg O19 Si24
• Calculated formula: C220 H350 Ge18 Hg O19 Si24
• Title of publication: {Ge9[Si(SiMe3)2(SiPh3)]3}(-): Ligand Modification in Metalloid Germanium Cluster Chemistry.
• Authors of publication: Kysliak, Oleksandr; Schrenk, Claudio; Schnepf, Andreas
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 14
• Pages of publication: 7083 - 7088
• a: 19.1052 ± 0.0019 Å
• b: 20.27 ± 0.002 Å
• c: 20.835 ± 0.002 Å
• α: 112.591 ± 0.002°
• β: 108.382 ± 0.002°
• γ: 103.66 ± 0.002°
• Cell volume: 6454.9 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0965
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.117
• Weighted residual factors for all reflections included in the refinement: 0.1394
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No