Information card for entry 4344028

Structure parameters

• Formula: C87 H118 N6 O24 Tb4
• Calculated formula: C87 H118 N6 O24 Tb4
• Title of publication: Tetranuclear and Pentanuclear Compounds of the Rare-Earth Metals: Synthesis and Magnetism.
• Authors of publication: Yadav, Munendra; Mondal, Abhishake; Mereacre, Valeriu; Jana, Salil Kumar; Powell, Annie K.; Roesky, Peter W.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 16
• Pages of publication: 7846 - 7856
• a: 13.9775 ± 0.0005 Å
• b: 17.7557 ± 0.0005 Å
• c: 21.8287 ± 0.0008 Å
• α: 68.762 ± 0.002°
• β: 85.665 ± 0.003°
• γ: 72.449 ± 0.002°
• Cell volume: 4811 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1727
• Residual factor for significantly intense reflections: 0.0815
• Weighted residual factors for significantly intense reflections: 0.1411
• Weighted residual factors for all reflections included in the refinement: 0.1652
• Goodness-of-fit parameter for all reflections included in the refinement: 0.902
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No