Crystallography Open Database

Information card for entry 4344609

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Coordinates	4344609.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Co8 H58 K5 Na2 O100 P2 W18
Calculated formula	Co8 K5 Na2 O100 P2 W18
Title of publication	Cobalt Clusters with Cubane-Type Topologies Based on Trivacant Polyoxometalate Ligands.
Authors of publication	Duan, Yan; Clemente-Juan, Juan M; Giménez-Saiz, Carlos; Coronado, Eugenio
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	2
Pages of publication	925 - 938
a	10.2222 ± 0.0003 Å
b	12.6115 ± 0.0004 Å
c	17.8646 ± 0.0006 Å
α	77.041 ± 0.003°
β	83.369 ± 0.003°
γ	73.088 ± 0.003°
Cell volume	2144.21 ± 0.12 Å³
Cell temperature	120 ± 0.1 K
Ambient diffraction temperature	120 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0855
Residual factor for significantly intense reflections	0.0519
Weighted residual factors for significantly intense reflections	0.1184
Weighted residual factors for all reflections included in the refinement	0.1428
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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