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Information card for entry 4344677
Preview
Coordinates | 4344677.cif |
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Original paper (by DOI) | HTML |
Formula | C39 H69 Ca N3 O Si2 |
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Calculated formula | C39 H69 Ca N3 O Si2 |
SMILES | [Ca]1(N([Si](C)(C)C)[Si](C)(C)C)([O]2CCCC2)N(C(=[N]1c1c(cccc1C(C)C)C(C)C)C(C)(C)C)c1c(cccc1C(C)C)C(C)C |
Title of publication | Amido Ln(II) Complexes Coordinated by Bi- and Tridentate Amidinate Ligands: Nonconventional Coordination Modes of Amidinate Ligands and Catalytic Activity in Intermolecular Hydrophosphination of Styrenes and Tolane. |
Authors of publication | Basalov, Ivan V.; Yurova, Olga S.; Cherkasov, Anton V.; Fukin, Georgy K.; Trifonov, Alexander A. |
Journal of publication | Inorganic chemistry |
Year of publication | 2016 |
Journal volume | 55 |
Journal issue | 3 |
Pages of publication | 1236 - 1244 |
a | 10.7194 ± 0.0003 Å |
b | 12.3082 ± 0.0002 Å |
c | 16.2806 ± 0.0005 Å |
α | 89.4044 ± 0.0019° |
β | 88.005 ± 0.003° |
γ | 82.382 ± 0.002° |
Cell volume | 2127.72 ± 0.1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0749 |
Residual factor for significantly intense reflections | 0.0496 |
Weighted residual factors for significantly intense reflections | 0.1288 |
Weighted residual factors for all reflections included in the refinement | 0.1387 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4344677.html
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