Information card for entry 4345546

Structure parameters

• Formula: C74 H69 B4 Co2 N19 O2 S
• Calculated formula: C74 H69 B4 Co2 N19 O2 S
• Title of publication: Reactions of Neutral Cobalt(II) Complexes of a Dianionic Tetrapodal Pentadentate Ligand: Cobalt(III) Amides from Imido Radicals.
• Authors of publication: Nurdin, Lucie; Spasyuk, Denis M.; Piers, Warren E.; Maron, Laurent
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 13.16 ± 0.003 Å
• b: 16.563 ± 0.003 Å
• c: 17.625 ± 0.004 Å
• α: 102.21 ± 0.03°
• β: 109.9 ± 0.03°
• γ: 94.97 ± 0.03°
• Cell volume: 3477.6 ± 1.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0625
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.0963
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No