Information card for entry 4345671

Structure parameters

• Formula: C22 H66 O Si10
• Calculated formula: C22 H66 O Si10
• Title of publication: Using Functionalized Silyl Ligands To Suppress Solvent Coordination to Silyl Lanthanide(II) Complexes.
• Authors of publication: Zitz, Rainer; Hlina, Johann; Aghazadeh Meshgi, Mohammad; Krenn, Heinz; Marschner, Christoph; Szilvási, Tibor; Baumgartner, Judith
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 9.3913 ± 0.0017 Å
• b: 13.142 ± 0.003 Å
• c: 16.586 ± 0.003 Å
• α: 90°
• β: 93.003 ± 0.003°
• γ: 90°
• Cell volume: 2044.2 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0787
• Weighted residual factors for significantly intense reflections: 0.162
• Weighted residual factors for all reflections included in the refinement: 0.1727
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No