Crystallography Open Database

Information card for entry 4345731

Preview

Coordinates	4345731.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H53 Cu2 N6 O23 V6
Calculated formula	C37 H53 Cu2 N6 O23 V6
Title of publication	Controllable Synthesis of Lindqvist Alkoxopolyoxovanadate Clusters as Heterogeneous Catalysts for Sulfoxidation of Sulfides.
Authors of publication	Li, Ji-Kun; Dong, Jing; Wei, Chuan-Ping; Yang, Song; Chi, Ying-Nan; Xu, Yan-Qing; Hu, Chang-Wen
Journal of publication	Inorganic chemistry
Year of publication	2017
Journal volume	56
Journal issue	10
Pages of publication	5748 - 5756
a	22.1519 ± 0.0006 Å
b	14.649 ± 0.0006 Å
c	18.5252 ± 0.0006 Å
α	90°
β	121.271 ± 0.002°
γ	90°
Cell volume	5138.1 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0635
Residual factor for significantly intense reflections	0.054
Weighted residual factors for significantly intense reflections	0.1688
Weighted residual factors for all reflections included in the refinement	0.1773
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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