Information card for entry 4345920

Structure parameters

• Formula: C32 H72 Cl2 Rh2 S4
• Calculated formula: C32 H72 Cl2 Rh2 S4
• Title of publication: Studies on the Activation and Hydrosilylation Catalysis of RhCl3(Bu2S)3.
• Authors of publication: Olsen, Matthew T.; Rekken, Brian D.; Eldred, Donald V.
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 13.5132 ± 0.001 Å
• b: 8.61 ± 0.0006 Å
• c: 19.7557 ± 0.0014 Å
• α: 90°
• β: 104.959 ± 0.001°
• γ: 90°
• Cell volume: 2220.7 ± 0.3 ų
• Cell temperature: 185 ± 2 K
• Ambient diffraction temperature: 185 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0641
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No