Information card for entry 4346042

Structure parameters

• Formula: C24 H28 Ge N2 O7 Ru2
• Calculated formula: C24 H28 Ge N2 O7 Ru2
• SMILES: CC(C)[N]1=C(c2ccccc2)N(C(C)C)[Ge](C(C)(C)C)([Ru]1(C#[O])(C#[O])C#[O])[Ru](C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Amidinatogermylene derivatives of ruthenium carbonyl: new insights into the reactivity of [Ru3(CO)12] with two-electron-donor reagents of high basicity.
• Authors of publication: Álvarez-Rodríguez, Lucía; Cabeza, Javier A.; García-Álvarez, Pablo; Pérez-Carreño, Enrique; Polo, Diego
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 6
• Pages of publication: 2983 - 2994
• a: 9.3494 ± 0.0001 Å
• b: 17.8506 ± 0.0002 Å
• c: 16.5316 ± 0.0002 Å
• α: 90°
• β: 90.475 ± 0.001°
• γ: 90°
• Cell volume: 2758.9 ± 0.05 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0285
• Weighted residual factors for significantly intense reflections: 0.0671
• Weighted residual factors for all reflections included in the refinement: 0.0729
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No