Information card for entry 4346213

Structure parameters

• Formula: C79 H74 Cl2 F12 P10 Pd2
• Calculated formula: C79 H74 Cl2 F12 P10 Pd2
• SMILES: [Pd]123[Pd]4([P](C[P]1(c1ccccc1)c1ccccc1)(CP(C[P]4(c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1)[P](C[P]2(CP(C[P]3(c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.ClCCl.[P](F)(F)(F)(F)(F)[F-].[P](F)(F)(F)(F)(F)[F-]
• Title of publication: Stepwise Expansion of Pd Chains from Binuclear Palladium(I) Complexes Supported by Tetraphosphine Ligands.
• Authors of publication: Tanase, Tomoaki; Hatada, Satoko; Noda, Sayo; Takenaka, Hiroe; Nakamae, Kanako; Kure, Bunsho; Nakajima, Takayuki
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 17
• Pages of publication: 8298 - 8309
• a: 12.3849 ± 0.0002 Å
• b: 12.3849 ± 0.0002 Å
• c: 50.5057 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7746.9 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 76
• Hermann-Mauguin space group symbol: P 41
• Hall space group symbol: P 4w
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for all reflections included in the refinement: 0.0963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No