Information card for entry 4346255

Structure parameters

• Formula: C76 H144 Bi12 K4 N8 Ni7 O28
• Calculated formula: C76 H144 Bi12 K4 N8 Ni7 O28
• Title of publication: [Bi12Ni7(CO)4](4-): Aggregation of Intermetalloid Clusters by Their Thermal Deligation and Oxidation.
• Authors of publication: Perla, Luis G.; Sevov, Slavi C.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 17
• Pages of publication: 8401 - 8405
• a: 15.7319 ± 0.0017 Å
• b: 25.995 ± 0.003 Å
• c: 16.6477 ± 0.0019 Å
• α: 90°
• β: 118.061 ± 0.0018°
• γ: 90°
• Cell volume: 6007.8 ± 1.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1135
• Residual factor for significantly intense reflections: 0.0632
• Weighted residual factors for significantly intense reflections: 0.1416
• Weighted residual factors for all reflections included in the refinement: 0.1703
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No